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Column Components

Column Components

In many operations like reaction, extraction & absorption, the transparency of glass is particular advantage. For such process a range of column components are available in Borosilicate glass which offers many advantages like:

  • Inert to almost all chemicals hence no risk of contamination.
  • Transparency allows visual monitoring of the process flow patterns, colour changes etc.
  • Almost universal resistance to corrosion
  • Smooth surface permits easy cleaning & prevents fouling.
COLUMN SECTIONS

Column can be constructed either by using pipesections with support plates or using column sections with packing supports.

Column sections are provided with fused shelf wherepacking support can rest.

Cat. Ref. DN L L1 Minimum packing Size Usual packing Size
CS3/1000 80 1000 75 9 12
CS4/1000 100 1000 75 12 15
CS6/1000 150 1000 75 15 25
CS6/1500 150 1500 75 15 25
CS9/1000 225 1000 100 20 25
CS9/1500 225 1500 100 20 15
CS12/1000 300 1000 100 25 25
CS12/1500 300 1500 100 25 25
CS16/1000 400 1000 150 25 25
CS16/1500 400 1500 150 25 15
CS18/1000 450 1000 150 25 25
CS18/1500 450 1500 150 25 25
CS24/1000 600 1000 200 40 40
COLUMN SECTIONS WITH THERMOMETER BRANCH

Above column sections can be provided with a thermometer branch below the packing shelf at 20° slope

Cat.Ref. DN DN1 L L1 d
CST3/1000 80 25 1000 125 50
CST4/1000 100 25 1000 125 75
CST6/1000 150 25 1000 125 125
CST6/1500 150 25 1500 125 125
CST9/1000 225 25 1000 150 175
CST9/1500 225 25 1500 150 175
CST12/1000 300 25 1000 150 250
CST12/1500 300 25 1500 150 250
CST16/1000 400 25 1000 200 250
CST16/1500 400 25 1500 200 350
CST18/1000 450 25 1000 200 400
CST18/1500 450 25 1500 200 400
CST24/1000 600 25 1000 250 540
PACKING SUPPORTS

Packing supports Type A are made of fused glass rods. Packing supports Type B (heavy duty) are made of glass plates vertically arranged and tied with PTFE tie rods

Cat.Ref. Size DN L Cross Section Area Max. Load Kgs. Minimum Packing Type
CP3* 80 10 45% 10 12 A
CP4* 100 12 50% 15 15 A
CP6* 150 15 55% 30 25 A
CP9* 225 19 60% 50 25 A
CP12* 300 19 65% 75 25 A
HD16 400 70 70% 150 25 B
HD18 450 70 70% 300 40 B
HD24 600 95 70% 300 40 B
PTFE PERFORATED PLATES

These are used as packing retainers to prevent the packing from lifting due to vapour velocity. These can be clamped between two components without using any gasket.

Cat.Ref. DN d L
TCP3 80 99 7
TCP4 100 132 9
TCP6 150 184 10
TCP9 225 254 12
TCP12 300 340 16
TCP16 400 463 25
TCP18 450 525 25
TCP24 600 689 30
SUPPORT PLATE ASSEMBLY

Support Plate Assembly can be coupled with apipe section (PS), so as to use the pipe section as a column section and to fill packings intoit. This system provides following advantages over the conventional system of using columnsection with a packing support.

  • Higher cross section area
  • More packing height.
  • No separate inventory of column sections.
  • Delivery period of pipe section are shorter.

This assembly consist of a glass support plate,a metal flange, a PTFE 'O' ring and nut-bolts.

Cat.Ref. DN L Cross Section Area Max. Load Kgs. Suitable Packing Size
LBE3* 80 25 70% 20 12
LBE4* 100 25 70% 30 15
LBE6* 150 50 70% 60 25
LBE9* 225 75 80% 90 25
LBE12* 300 75 80% 150 25
Packings require for various pipe sections (Kgs.)
Pipe Section
Vol(L) FC FC 12 FC 15 FC 25 FCB 40 FCB 50
PS3/1000 5 3 3 2 - - -
PS4/1000 8 - 4 3 3 - -
PS6/1000 18 - 9 7 7 - -
PS9/1000 37 - - 15 15 15 -
PS12/1000 66 - - 17 30 25 -
PS16/1000 125 - - - 65 50 53
PS18/1000 165 - - - 90 65 70
PS24/1000 295 - - - - 115 125
Notes of use of Column Packing
  • Due to their low bulk densities, Glass Raschig rings are particularly suitable for packing glass columns
  • Generally, the ratio of Column diameter to packing diameter should not be less than 8:1
  • When using smaller packing size, a small layer of larger packing should be used on packing support, to prevent the smaller packing falling through.
  • In vacuum application and applications involving high vapour velocities, packing may b e lifted and may damage to other parts. To prevent this, a packing retainer (PTFE p e rfo ra t e d plates) should be used above the packed section.
COLUMN PACKING-RASCHIG RINGS

Raschig rings upto 25mm are also available in Neutral glass. 20mm, 30mm, 40mm and 50mm are available in Borosilicate glass 3.3.

Cat.Ref. Size Bulk Density Kg/Ltr Specific Surface m2 /m3 Glass
FC8 8x8 0.6 500 Neutral
FC9 9x9 0.6 500 Neutral
FC12 12x12 0.5 400 Neutral
FC15* 15x15 0.4 300 Neutral
FC25* 25x25 0.35 250 Neutral
FCB20 20x20 0.33 300 Borosilicate
FCB30 30x30 0.27 180 Borosilicate
FCB40 40x40 0.22 160 Borosilicate
FCB50 50x50 0.19 120 Borosilicate
PALL RINGS

Pall Rings are also available for column packing as per below specification

Cat.Ref. Size Bulk Density Kg/Ltr Specific Surface m2 /m3 Glass
FCP30 30x30 0.38 234 Borosilicate
FCP40 40x40 0.32 D 187 Borosilicate
FCP50 50x50 0.26 140 Borosilicate
COLUMN FEED PIPE

Feed pipe directs the process fluidto the centre of the column.

Cat.Ref. DN DN1 DN2 L d
FP3 80 25 25 100 12
FP4 100 25 25 125 12
FP6 150 40 25 150 19
FP9 225 40 25 175 19
FP12 300 40 25 225 19
FP16 400 40 25 275 19
FP18 450 40 25 300 19
FP24 600 50 40 450 25

DN refers the nominal diameter of the column

COLUMN FEED SPARGERS

In column feed spargers, holes are provided at three sides of pipe

Cat.Ref. DN DN1 DN2 L Holes
SPG3 80 25 25 125 21x2mm
SPG4 100 25 25 150 21x2mm
SPG6 150 40 25 200 27x2mm
SPG9 225 40 25 275 27x2mm
SPG12 300 40 25 350 30x3mm
SPG16 400 40 25 450 39x3mm
SPG18 450 40 25 500 39x3mm
SPG24 600 50 40 650 60x3mm

DN refers the nominal diameter of the column.

SPRAY FEED SECTION

Spray feed section are provided with circular tube having holes at the bottom.

Cat.Ref. DN DN1 L L1 Holes
FR3 80 25 200 100 21x2mm
FR4 100 25 250 125 21x2mm
FR6 150 40 250 125 27x2mm
FR9 225 40 250 125 27x2mm
FR12 300 40 300 150 30x3mm

For bigger columns, Spray feed pipe withUnequal Tee should be used.

SPRAY FEED PIPES

Spray feed pipes are provided with oval tubehaving holes at the bottom. These should be usedwith unequal tees.

Cat.Ref. DN DN1 DN2 L L1 Holes Size Tee Suitable
FD6 150 80 25 225 125 27x2mm PTU6/3
FD9 225 100 25 25 150 27x2mm PTU9/4
FD12 300 150 25 400 200 30x3mm PTU12/6
FD16 400 150 50 500 200 39x3mm PTU16/6
FD18 450 150 50 550 200 39x3mm PTU18/6
FD24 600 150 50 700 200 60x3mm PTU24/6

DN refers the nominal diameter of the column.

PTFE REDISTRIBUTORS

PTFE redistributors are used to prevent channeling incolumns. These can be clamped between twocomponents without using any gasket

Cat.Ref. DN d L
TL3 80 55 20
TL4 100 80 20
TL6 150 100 20
TL9 225 175 22
TL12 300 215 25
TL16 400 315 25
TL18 450 365 30
L24 600 420 30
COLUMN ADAPTORS

Cat. Ref.

DN

DN1

DN2

L

L1

L2

 CA3/1/1

80

25

25

150

75

100

 CA3/1.5/1

80

40

25

175

100

100

 CA3/2/1

80

50

25

175

100

100

 CA4/1/1

100

25

25

150

75

125

 CA4/1.5/1

100

40

25

175

100

125

 CA4/2/1

100

50

25

225

125

125

 CA4/3/1

100

80

25

225

125

125

 CA6/1/1

150

25

25

200

100

150

 CA6/1.5/1

150

40

25

200

100

150

 CA6/2/1

150

50

25

250

125

150

 CA6/3/1

150

80

25

250

150

150

 CA6/4/1

150

100

25

275

150

175

 CA9/1.5/1.5

225

40

40

250

150

175

 CA9/2/1.5

225

50

40

250

150

175

 CA9/3/1.5

225

80

40

300

175

200

 CA9/4/1.5

225

100

40

350

175

200

 CA9/6/1.5

225

150

40

400

200

250

 CA12/1.5/1.5

300

40

40

300

150

225

 CA12/2/1.5

300

50

40

300

150

225

 CA12/3/1.5

300

80

40

300

150

250

 CA12/4/1.5

300

100

40

350

175

250

 CA12/6/1.5

300

150

40

425

225

250

 CA12/9/1.5

300

225

40

450

225

300

 CA16/2/2

400

50

50

400

200

300

 CA16/3/2

400

80

50

450

250

300

 CA16/4/2

400

100

50

450

250

300

 CA16/6/2

400

150

50

550

300

350

 CA16/9/2

400

225

50

550

300

350

 CA18/2/2

450

50

50

400

200

325

 CA18/3/2

450

80

50

450

250

350

 CA18/4/2

450

100

50

450

250

350

 CA18/6/2

450

150

50

550

300

350

 CA18/9/2

450

225

50

550

300

400

 CA18/12/2

450

300

50

750

400

400

 CA24/2/2

600

50

50

450

200

400

 CA24/3/2

600

80

50

500

250

400

 CA24/4/2

600

100

50

500

250

400

 CA24/6/2

600

150

50

650

300

450

 CA24/9/2

600

225

50

650

300

450

 CA24/12/2

600

300

50

800

400
500

Column adaptors with DN2 of different size(maximum equaling to DN1) can be manufactured with the same dimensions.

FLAT TOP COLUMN ADAPTORS

These are generally used as headersof shell and tube heat exchangersand columns.

Cat.Ref.

DN

DN1

L

L1

CA3/1

80

25

100

75

CA3/1.5

80

40

125

100

CA4/1

100

25

100

75

CA4/1.5

100

40

125

100

CA6/1

150

25

150

100

CA6/1.5

150

40

150

100

CA6/2

150

50

200

125

CA6/3

150

80

200

150

CA9/1.5

225

40

200

150

CA9/2

225

50

200

150

CA9/3

225

80

250

175

CA9/4

225

100

250

175

CA12/2

300

50

250

150

CA12/3

300

80

250

150

CA12/4

300

100

300

175

CA12/6

300

150

350

225

Cat.Ref. DN DN1 DN2 L L1 L2 L3 L4 L5
CAM4/2/1/1 100 50 25 450 300 150 200 125 125
CAM6/3/1/1 150 80 25 450 300 150 200 150 150
CAM9/3/1/1 225 80 25 450 300 150 200 175 200
CAM12/3/1/1 300 80 25 450 300 150 200 225 250
REFLUX DIVIDERS
Manually Operated

Reflux dividers are used to take off the distillatefrom the column. Usually a valve is to be fitted ondistillate outlet which controls the reflux coarsely.

Cat.Ref. DN DN1 DN2 L L1 Free Corss Section Cm2 Max. Product L/hr
RDA3* 80 25 25 200 100 20 300
RDA4* 100 25 25 250 150 50 500
RDA6* 150 25 25 250 150 100 700
RDA9* 225 25 25 375 150 150 900
RDA12* 300 25 25 375 150 250 1100
RDA16 400 40 40 500 200 350 1300
RDA18 450 40 40 600 275 500 1500

DN2 is used for insertion of a thermometer pocket. A bellow is recommended on the distillate outlet DN1.

Magnetically Operated

These reflux dividers are to be used with a electro -magnet and a timer. These have a swinging funnel machanism which is operated magnetically from outside to remove the condensate or to return the reflux. Through this, correct control of reflux-ratio is possible. Funnel remains at 100% reflux position while magnet is inactive

Cat.Ref. DN DN1 DN2 L L1 Free Corss Section Cm2 Max. Product L/hr
RHM3 80 25 25 375 75 20 90
RHM4 100 25 25 400 75 50 180
RHM6 150 25 25 450 100 100 300
RHM9 225 25 25 550 100 150 500
RHM12 300 25 25 700 100 250 650
RHM16 400 40 40 800 150 350 1000
RHM18 450 40 40 900 150 500 1300

DN2 is used for insertion of a Thermometer Pocket. A liquid seal is recommended on the distillate outlet ofthis reflux divider to prevent the vapour passing directly to the receiver.

PNEUMATIC REFLUX DIVIDER
Cat.Ref. DN DN1 DN2 L
RPH3 80 25 25 250
RPH4 100 25 25 250
RPH6 150 40 25 250
RPH9 225 40 50 375
RPH12 300 40 50 375
THERMOMETER POCKETS FOR REFLUX DIVIDER

These thermometer pockets are tobe used with reflux dividers orcolumn sections. DN refers to thenominal diameter of the Refluxdivider or Column.

Cat.Ref. DN DN1 d L
TP3* 80 25 12 75
TP4* 100 25 12 100
TP6* 150 25 12 125
TP9* 225 25 12 150
TP12* 300 25 12 200
TP16 400 40 19 250
TP18 450 40 19 300
LIQUID SEALS

Liquid seals are to be fitted onthe distillate outlet ofmagnetically operated reflux divider. This prevent the passing of vapourdirectly to the receiver

Cat.Ref. DN DN1 L Type
LS1* 25 25 200 A
LS1.5 40 25 300 A
LSV1 25 - 200 B
COLUMN SECTION WITH INBUILT
PACKING SUPPORT

Surya introduce single piece column section with inbuilt packing supportr

Advantages of this column against conventional column section:
  • Ease in installation being a single piece instead of two pieces
  • There is no need to maintain stock of CS and packing support
  • Increases effective packed height which results in to increase in efficiency.
  • Zero maintenance against column flooding.
Cat.Ref. DN D d L Max Load Kgs Suitable Packing Size
CSP3/1000 80 10 10 1000 20 12
CSP4/1000* 100 10 14 1000 30 15
CS6P/1000* 150 12 22 1000 60 25
CSP9P/1000* 225 12 22 1000 90 25
CSP12/1000* 300 12 22 1000 150 25
DIGITAL TEMPERATURE INDICATOR

These are generally used as headersof shell and tube heat exchangersand columns.

This instrument is mainly used to monitor the temperature of liquid in a glass vessel in a typical Glass Distillation Unit.

The instrument consists of a Temperature indicator and a Resistance Temperature Detectors (RTD). The instrument works on 230V, 50Hz power supply. This displays the temperature in degree Centigrades in three and half digits of 12.5mm character height.

Cat.Ref. Vessel size RTD Length
DTI20 20 400
DTI50 50 500
DTI100 100 600
DTI200 200 700
ELECTRO-MAGNETS

Electro - magnets are used to operate Magnetically operated Reflux dividers. When 'On ' t h e magnet attracts the swinging funnel of the reflux divider so that distillate can be taken off.

Electro-magnets are to be mounted outside the glass column, just near to the reflux divider, with the help of adjustable fittings. These are designed to use with Timers to maintain correct ratio between 'Off' and 'On' timings of its activation

Electro-magnets work on 220V DC power supply, for which a output socket is provided in the Timers.

Cat.Ref. Type
RPM Non-flameproof
RPF Flameproof
TIMERS

Timers are designed to use with Electro- magnets to provide a correct ratio of refluxand distillate when operating a Magnetically operated reflux divider.

Timers work on a power supply of 230V, 50Hz.

Cat.Ref. Type
QRT Flameproof